In this paper, a new device of synthesizing iodoform by electrochemistry method was introduced and the optimum reaction condition of synthesizing iodoform had been explored by this device. 对电化学合成碘仿装置进行了改进,探索出了利用该装置合成碘仿的最佳反应条件。
The p-ethylacetophenone was synthesized with acetylated, ethylbenzene and anhydrous aluminium chloride, then was oxidized top-ethylbenzoic acid with iodoform reaction. 以乙酸酐、乙基苯和无水三氯化铝为原料合成对乙基苯乙酮,并利用碘仿反应氧化对乙基苯乙酮制备对乙基苯甲酸。
The improvement of the device on synthesizing iodoform by electrochemistry method and the exploring of reaction conditions 电化学合成碘仿装置的改进及反应条件的探索